Portable Handheld LIBS Spectrometers SCIAPSCarbon LIBS Analyzer Z-902C SCIAPS

The key to rock solid, in-field carbon analysis for alloys.

• Identification of stainless steels and low alloy steels, including carbon analysis down to 70 ppm and instant CE (carbon equivalents) calculations.
• Powerful laser, on-board argon purge and high resolution spectrometer are built for carbon.
• Narrow profile for accessing the tightest spaces, aerospace-grade aluminum body for improved performance in high ambient temperatures, and re-designed user-interface. The most usable platform on the market, at only 4.35 lbs. (1.97 kg).

Spectrometer range 190 nm – 420 nm. Includes a second, dedicated spectrometer for superior resolution in the 190 – 230 nm range for carbon.

PMI and NDT
Confirm alloy type and grade 300 series stainless steels into L, H, and S series. Carbon equivalent for welding. Material verification pre- and post-fabrication. Validating mill test reports. Material verification in chemical plants and refineries. Re-rating vessels.

Pipeline integrity management
Grading. Determining carbon equivalents. Validating MTRs.

Steel production
Screen incoming scrap material. In-process quality control. Resolving material mix-ups. Rapid screening of material at EAF for heat compliance.

The essentials for Carbon Analysis in Alloy with Handheld LIBS

1. High-purity Argon and Purge
   Argon purge is essential for quantitative analysis with LIBS and OES, and for carbon it’s critical. SciAps patented Opti-Purge technique is a key component for measuring carbon accurately. Opti-Purge delivers argon exactly where it’s needed and uses about 1,000 times less argon than a spark OES, allowing for a user-replaceable canister. Operators can analyze up to 600 samples with the argon canister for most alloy testing, and 125-200 samples for carbon analysis.
2. High laser Pulse Energy and Frequency
   The SciAps laser delivers 5-6 mJ/pulse on the sample, with a 50 Hz repetition rate. As any user of spark OES knows, sample prep is critical for carbon analysis—a good grind and a good pre-burn are as critical for LIBS as for spark OES. SciAps high energy and high rep rate laser (50 Hz) rapidly burns off surface contamination in order to provide a good analysis.
3. Laser Raster
   Rastering is critical for accurate carbon tests with LIBS. The Z moves the laser to 6 distinct locations and analyzes each spot for 0.5 seconds for every 3-second test. The laser is typically 50 um diameter beam. On that scale, micro inclusions in the alloys and the grain structure of the alloy can impact the analysis. By averaging across six unique locations, the system collects data that is representative of the alloy, not just an individual location.
4. Analysis Averaging
   Multi-shot averaging and data rejection are critical to getting the best carbon tests. The combination of these two features, known as analysis averaging, allows the operator to (optionally) reject test data with significant point-by-point discrepancies then automatically create a final result.
5. Micro-Camera and LED Spotlight
   Proper alignment is critical to getting good analysis. Take out the guess work with SciAps micro-camera and LED Spotlight. The camera shows the sample in high resolution and ensures that the instrument is positioned correctly; LED Spotlight shows exactly where the laser will burn the sample. Get a good burn every time.
6. Argon: Cost of Operation
   Argon costs just pennies per test, far less expensive than spark OES and much more convenient.  What does that mean in real terms? It depends if you are doing carbon tests or general alloy tests.  You can expect to get about 100 tests per canister for carbon, and 600 tests for general alloy.